HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86656593, compound → HCID 44230391, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86656593 | HCID 86656593 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 44230391 | HCID 44230391 | 103.3% |
Reaction Steps
A mixture of 110 mg N2-methyl-N6-(tetrahydro-2H-pyran-2-yloxy)-3,4-dihydroisoquinoline-2,6(1H)-dicarboxamide in 4 ml methanol and 6 ml 0.1M aqueous HCl is stirred for 16 h and evaporated. The residue is dissolved in acetonitrile and water and lyophilized. 85 mg of colorless foam are obtained. MH+=250.2
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08575193B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-3913879ef882468aa02d59b5a571637d |
| Source note | uspto-grants-2013_11 |