HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 44229351, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86656603 | HCID 86656603 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 44229351 | HCID 44229351 | 36.2% |
Reaction Steps
A mixture of 150 mg of 2-acetyl-N-(tetrahydro-2H-pyran-2-yloxy)-1,2,3,4-tetrahydroisoquinoline-6-carboxamide, 1 ml methanol and 1.5 ml of an aqueous, 0.1 N hydrochloric acid is stirred for 3 h at ambient temperature. The reaction mixture is lyophilized. 40 mg of the title compound are obtained as colorless oil. MH+=235.0
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08575193B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-e6aa51618d304ac99a3d3cb397a84078 |
| Source note | uspto-grants-2013_11 |