HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2,2-Trifluoroethyl trifluoromethanesulfonate → 5-Bromo-1-(2,2,2-trifluoroethyl)pyridin-2(1H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2,2-Trifluoroethyl trifluoromethanesulfonate | HCID 80366 | — |
| Reactant | 5-Bromo-2-hydroxypyridine | HCID 599528 | — |
| Product | 5-Bromo-1-(2,2,2-trifluoroethyl)pyridin-2(1H)-one | HCID 53408099 | — |
Reaction Steps
5-bromo-1-(2,2,2-trifluoroethyl)pyridin-2(1H)-one was prepared from 5-bromopyridin-2(1H)-one and 2,2,2-trifluoroethyl trifluoromethanesulfonate following a procedure analogous to that described in Example 628 Step 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08575156B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-be28a48766f947149316cfaf1b0b33be |
| Source note | uspto-grants-2013_11 |