1,4-Dioxane hydrochloride → HCID 68379297, compound

Participants

Reaction Steps

((S)-1-{1-[6-(1H-pyrazol-4-yl)-pyridazin-3-yl]-cyclopropylcarbamoyl}-ethyl)-carbamic acid tert-butyl ester was dissolved in CH2Cl2 (1.0 mL) and 4M HCl dioxane (2 mL, 8 mmol) was added. After 1.5 h, the solvents were removed at 50° C. under a stream of N2. This material was dried under vacuum to yield 73 mg of the title compound, m/z 273.5 [M+H]+.

Provenance & Evidence