Sodium Carbonate → Chromium(3+) carbonate (2/3)
Reaction equation
[C:1](=[O:4])([O-:3])[O-:2].[K+].[K+].[C:7](=[O:10])([O-:9])[O-:8].[Na+].[Na+].[Cl-].[Cr+3:14].[Cl-].[Cl-]>>[C:1](=[O:2])([O-:4])[O-:3].[Cr+3:14].[C:7](=[O:8])([O-:10])[O-:9].[C:1](=[O:2])([O-:4])[O-:3].[Cr+3:14]Participants
4
Procedure
731 g of a 20% aqueous solution of potassium carbonate was used instead of the 10% aqueous solution of sodium carbonate used in Example 1, and was simultaneously added with chromium chloride at an addition speed of 14.6 g/min. The pH of the reaction liquid was maintained at about 8. Except these, a light blue chromium (III) carbonate powder was obtained as in Example 1. Measurement as in Example 1 was performed for the obtained chromium (III) carbonate. The results are shown in the following Table 1.
Workup
- customThe pH of the reaction liquid
- temperaturewas maintained at about 8
Sources & evidence
- ORD record
- ord-5a89cece13dd413683313b65e477192f
- Source dataset
- uspto-grants-2013_11
- Patent number
- US08580221B2
Reaction notes
Loading…