Hydrochloric Acid → HCID 59484923, compound

Participants

Reaction Steps

90 mg (0.17 mmol) of tert-butyl 4-(2-{3-[3-(1-methyl-1H-pyrazol-4-yl)-6-oxo-6H-pyridazin-1-ylmethyl]phenyl}pyrimidin-5-yl)piperazine-1-carboxylate are dissolved in 10 ml of dioxane, and 1 ml of 4 N HCl in dioxane is added. The reaction mixture is stirred at room temperature for 15 h and subsequently evaporated to dryness; yield: 80 mg of “A292” hydrochloride; HPLC: 2.05 min (method C); LC-MS: 429 (M+H).

Provenance & Evidence