HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropanemethanamine → HCID 57855949, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropanemethanamine | HCID 75646 | — |
| Reactant | HCID 57855896 | HCID 57855896 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 57855949 | HCID 57855949 | 74% |
Reaction Steps
0.55 g (1.15 mol) 9-chloro-2-[2-(3-chloro-pyridin-2-yl)-5-trifluoromethyl-2H-pyrazol-3-yl]-3-oxa-1,5,8-triaza-anthracen-4-one and 0.5 ml C-cyclopropylmethylamine is dissolved in 15 ml THF and stirred for 8 hours. After evaporation, the residue is crystallised in diethyl ether to give 0.47 g (74%) of the title compound. m.p.: 180-183° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580785B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-a1e971d9561c4b428b2b732cb225479f |
| Source note | uspto-grants-2013_11 |