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HRID2039610

反应详情

EQUATION

反应方程式

HRID 2039610 的结构方程式

REACTANTS

反应物

2
结构：CN
HCID6329

Methylamine

CH5N

结构：O=c1oc(-c2cc(C(F)(F)F)nn2-c2ncccc2Cl)nc2c(Cl)c3nsnc3cc12
HCID57855908

未命名化合物

PRODUCTS

生成物

1
结构：CNC(=O)c1cc2nsnc2c(Cl)c1NC(=O)c1cc(C(F)(F)F)nn1-c1ncccc1Cl
HCID57855936

未命名化合物

PROCEDURE

实验过程

See step f) of Example H2 using 4-chloro-6-[2-(3-chloro-pyridin-2-yl)-5-trifluoromethyl-2H-pyrazol-3-yl]-7-oxa-2-thia-1,3,5-triaza-cyclopenta[b]naphthalen-8-one as starting material and methylamine (40% in H2O). After overnight reaction and chromatography column purification, a slightly brown solid is obtained (75%). LC/MS: 538/539 (M+Na)+.

WORKUP

后处理

  1. customAfter overnight reaction and chromatography column purification
  2. customa slightly brown solid is obtained (75%)