HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 57855911, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 136174558 | HCID 136174558 | — |
| Product | HCID 57855911 | HCID 57855911 | 26% |
Reaction Steps
See example H3 using 4-chloro-6-[2-(3-chloro-pyridin-2-yl)-5-trifluoromethyl-2H-pyrazol-3-yl]-1H-7-oxa-1,3,5-triaza-cyclopenta[b]naphthalen-8-one as starting material and 3 equivalents of methylamine (40% in H2O). A white solid is obtained within 26% yield. m.p.: 190-192° C.; LC/MS: 498/500 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580785B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-3b95f614844d484f90a32dedaf3f6e54 |
| Source note | uspto-grants-2013_11 |