HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2039700Generated: October 25, 2026
(3-Methylbutyl)hydrazine → HCID 58266285, compound
https://huagongshe.com/reaction/2039700
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | (3-Methylbutyl)hydrazine | HCID 18696583 | — |
| Reactant | HCID 58266264 | HCID 58266264 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 58266285 | HCID 58266285 | — |
Reaction Steps
150 mg (0.295 mmol) of the compound from Example 6A were dissolved in 3 ml of dioxane, and 91 mg (0.885 mmol) of (3-methylbutyl)hydrazine were added. The mixture was stirred at 120° C. for 3 h and then concentrated. The residue was taken up in DMSO and purified by preparative HPLC (Method 10). This gave 43 mg (29% of theory) of the target compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08580800B2 |
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| Source dataset | uspto-grants-2013_11 |
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| ORD ID | ord-be4d04f3973a45b0b4fd368f7ecbe6d9 |
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| Source note | uspto-grants-2013_11 |
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