HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-N-methylbenzamide → HCID 58327706, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-N-methylbenzamide | HCID 676526 | — |
| Reactant | HCID 86654847 | HCID 86654847 | — |
| Product | HCID 58327706 | HCID 58327706 | — |
Reaction Steps
N-Methyl-3-((5-(2-methylbenzoyl)-7H-pyrrolo[2,3-d]pyrimidin-4-yl)amino)benzamide was synthesized using 3-amino-N-methylbenzamide and ((4-chloro-7H-pyrrolo[2,3-d]pyrimidin-5-yl)(o-tolyl)methanone according to the general procedure A. An off-white solid was obtained. M.p.>300° C.; 400 MHz 1HNMR (DMSO-d6) δ 11.47 (s, 1H), 8.48-8.47 (m, 2H), 8.24-8.20 (m, 2H), 7.60 (s, 1H), 7.52-7.45 (m, 4H), 7.40-7.32 (m, 2H), 2.86 (d, J=4.4 Hz, 3H), 2.34 (s, 3H); LCMS [M+H] 386.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580803B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-c3a58b6433824a9da15288da1504dc8c |
| Source note | uspto-grants-2013_11 |