HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70840036, compound → HCID 25095370, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70840036 | HCID 70840036 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 25095370 | HCID 25095370 | — |
Reaction Steps
Pd/C (50 mg) is added to a solution of 2-(2-cyano-vinyl)-pyrazolo[1,5-a]pyridine-4-carboxylic acid (adamantan-1-ylmethyl)-amide in MeOH. The mixture is stirred under hydrogen balloon for 6 h. The mixture is filtered through celite and the celite and solvent are removed to give the title compound. LC-MS m/z (M+H+): 363.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580812B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-fcb6bed4dbb54e549007aca2ea6b73da |
| Source note | uspto-grants-2013_11 |