HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86651085, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86651086 | HCID 86651086 | — |
| Reactant | HCID 87206065 | HCID 87206065 | — |
| Product | HCID 86651085 | HCID 86651085 | 35.1% |
Reaction Steps
The compound of step 1 (30 mg, 53 μmol) was reacted analogously as described in example 4, step 2. Dissolution of the obtained solid in a small quantity of MOH, addition of hydrochloric acid (0.1 M) and lyophilization overnight yielded 8.6 mg of the title compound in the form of the [7-chloro-2-(3-fluoro-2-methyl-benzyl)-1-phenyl-1H-pyrrolo[2,3-c]pyridin-3-yl]-piperazin-1-yl-methanone dihydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580813B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-99c4bd97401f4948b03ae47d79014ae7 |
| Source note | uspto-grants-2013_11 |