HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 56678527, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 66922273 | HCID 66922273 | — |
| Reactant | HCID 66922280 | HCID 66922280 | — |
| Product | HCID 56678527 | HCID 56678527 | 89.3% |
Reaction Steps
The compound of step 1 (40 mg, 61 μmol) was reacted analogously as described in example 4, step 2. Dissolution of the obtained solid in a small quantity of MOH, addition of hydrochloric acid (0.1 M) and lyophilization overnight yielded 30 mg of the title compound in the form of the [2,7-bis-(3-fluoro-2-methyl-benzyl)-1-phenyl-1H-pyrrolo[2,3-c]pyridin-3-yl]-piperazin-1-yl-methanone dihydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580813B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-65a57e9571fa467585109c858cf78398 |
| Source note | uspto-grants-2013_11 |