HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 56671819, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 66922268 | HCID 66922268 | — |
| Reactant | HCID 66922282 | HCID 66922282 | — |
| Product | HCID 56671819 | HCID 56671819 | 50.3% |
Reaction Steps
The compound of step 1 (29 mg, 52 μmol) was reacted analogously as described in example 4, step 2. Dissolution of the obtained solid in a small quantity of MOH, addition of hydrochloric acid (0.1 M) and lyophilization overnight yielded 12 mg of the title compound in the form of the [7-ethyl-2-(5-fluoro-2-methyl-phenoxy)-1-phenyl-1H-pyrrolo[2,3-c]pyridin-3-yl]-piperazin-1-yl-methanone dihydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580813B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-a3af2ffbd9524a138e6f7084d7ca2434 |
| Source note | uspto-grants-2013_11 |