HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66922212, compound → HCID 66922112, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66922212 | HCID 66922212 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 66922112 | HCID 66922112 | 94.6% |
Reaction Steps
The compound of step 1 (5.6 g, 24.5 mmol) and palladium on charcoal (1.12 g, 10%) were stirred in ethanol (160 ml) under a hydrogen atmosphere for 3 h. The catalyst was filtered off and the solvent removed in vacuo to give 5.34 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580813B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-c23e80ff739b47988f3c9e4501c4eaa0 |
| Source note | uspto-grants-2013_11 |