HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 56672057, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 66922340 | HCID 66922340 | — |
| Reactant | HCID 66922358 | HCID 66922358 | — |
| Product | HCID 56672057 | HCID 56672057 | 15.4% |
Reaction Steps
The compound of step 3 (19 mg, 35 μmol) was reacted analogously as described in example 1, step 7. Dissolution of the obtained solid in a small quantity of MOH, addition of hydrochloric acid (0.1 M) and lyophilization overnight yielded 2.4 mg of the title compound in the form of the [2-(5-fluoro-2-methyl-phenoxy)-6-methyl-1-phenyl-1H-pyrrolo[3,2-b]pyridin-3-yl]-piperazin-1-yl-methanone dihydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580813B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-3640038e8cf5413c9a1e18faef4c2691 |
| Source note | uspto-grants-2013_11 |