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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2039867Generated: October 31, 2026

Hydrochloric Acid → HCID 56665121, compound

https://huagongshe.com/reaction/2039867

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
Reactant2,6-DimethylphenolHCID 11335—
ReactantHCID 66922105HCID 66922105—
ReactantHCID 66922346HCID 66922346—
ProductHCID 56665121HCID 56665121—

Reaction Steps

The compound of step 7 (28 mg, 57.7 μmol) and 2,6-dimethylphenol were reacted analogously as described in example 1, step 6, and the product subsequently reacted as described in example 1, step 7. The obtained solid was dissolved in a small quantity of MOH, mixed with hydrochloric acid (0.1 M) and lyophilized overnight to give 15 mg of the title compound in the form of the [2-(2,6-dimethyl-phenoxy)-6-ethoxy-1-phenyl-1H-pyrrolo[3,2-b]pyridin-3-yl]-piperazin-1-yl-methanone dihydrochloride.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08580813B2
Source datasetuspto-grants-2013_11
ORD IDord-39dc75013ba14ef28ccbcc87f5250bc7
Source noteuspto-grants-2013_11