HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 56665121, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2,6-Dimethylphenol | HCID 11335 | — |
| Reactant | HCID 66922105 | HCID 66922105 | — |
| Reactant | HCID 66922346 | HCID 66922346 | — |
| Product | HCID 56665121 | HCID 56665121 | — |
Reaction Steps
The compound of step 7 (28 mg, 57.7 μmol) and 2,6-dimethylphenol were reacted analogously as described in example 1, step 6, and the product subsequently reacted as described in example 1, step 7. The obtained solid was dissolved in a small quantity of MOH, mixed with hydrochloric acid (0.1 M) and lyophilized overnight to give 15 mg of the title compound in the form of the [2-(2,6-dimethyl-phenoxy)-6-ethoxy-1-phenyl-1H-pyrrolo[3,2-b]pyridin-3-yl]-piperazin-1-yl-methanone dihydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580813B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-39dc75013ba14ef28ccbcc87f5250bc7 |
| Source note | uspto-grants-2013_11 |