HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 68756964, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Methyl 5-amino-1H-pyrrolo[2,3-b]pyridine-2-carboxylate | HCID 40152010 | — |
| Product | HCID 68756964 | HCID 68756964 | 55.4% |
Reaction Steps
The compound is prepared according to the protocol described in example A (stage 2) using 200 mg (1.04 mmol) of methyl 5-amino-1H-pyrrolo[2,3-b]pyridine-2-carboxylate and 121 μL (1.04 mmol) of benzoyl chloride instead of cyclopropanecarbonyl chloride. After treatment, 170 mg of beige solid is obtained (55%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580815B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-b50f91d4afa84744afb57697ebd29bed |
| Source note | uspto-grants-2013_11 |