HuagongsheHuagongshe Chemistry Print Report · For research reference only
Vanillin → 4-(2-Chloro-4-cyanophenoxy)-3-methoxybenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Vanillin | HCID 1183 | — |
| Reactant | 3-Chloro-4-fluorobenzonitrile | HCID 145525 | — |
| Product | 4-(2-Chloro-4-cyanophenoxy)-3-methoxybenzaldehyde | HCID 51051501 | — |
Reaction Steps
4-(2-Chloro-4-cyanophenoxy)-3-methoxybenzaldehyde was prepared from vanillin and 3-Chloro-4-fluorobenzonitrile following General Procedure A. 1H NMR (400 Hz, CDCl3) δ 9.95 (s, 1H), 7.76 (d, 1H), 7.56 (br s, 1H), 7.50 (d, 1H), 7.45 (brd, 1H), 7.15 (d, 1H), 6.78 (d, 1H), 3.90 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580832B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-884de01f6656428abfc91a8821b7f9b2 |
| Source note | uspto-grants-2013_11 |