HRID2040157

反应详情

EQUATION

反应方程式

HRID 2040157 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

N-Benzyl-1,1-dioxotetrahydro-2H-thiopyran-4-amine (2.00 g) was added to ethanol (40 mL) in a pressure bottle. Palladium hydroxide on carbon (0.587 g) was added and the solution was stirred under 30 psi of hydrogen at room temperature for 2 hours. The mixture was filtered though a nylon membrane and the solvent was removed under vacuum.

WORKUP

后处理

  1. filtrationThe mixture was filtered though a nylon membrane
  2. customthe solvent was removed under vacuum