HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosuccinimide → HCID 67169326, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | HCID 67127242 | HCID 67127242 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 67169326 | HCID 67169326 | — |
Reaction Steps
A mixture of EXAMPLE 388C (0.15 g) and N-chlorosuccinimide (0.081 g) in CH3CN (8 mL) was heated at 90° C. for 16 hours. The solvent was removed, and the residue was purified by flash column chromatography on silica to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580794B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-501b2a4e78414fda8e95c78bec89897d |
| Source note | uspto-grants-2013_11 |