HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzosuberone → 9-Methoxy-5,6,7,12-tetrahydro-benzo[6,7]cyclohepta[1,2-b]indole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzosuberone | HCID 70003 | — |
| Reactant | 4-Methoxyphenylhydrazine hydrochloride | HCID 2723904 | — |
| Product | 9-Methoxy-5,6,7,12-tetrahydro-benzo[6,7]cyclohepta[1,2-b]indole | HCID 59676037 | — |
Reaction Steps
Following the procedure described in Example 4, using 6,7,8,9-tetrahydro-benzocyclohepten-5-one (1.10 g, 6.87 mmoL) and 4-methoxy-phenylhydrazine HCl salt (1.20 g, 6.87 mmoL) as the starting material, the title compound was prepared as a brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580840B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-e9db6d984be14b66bc39d1b76dc85d2f |
| Source note | uspto-grants-2013_11 |