HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67026905, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2-(1-Ethylpropyl)-6-methylisonicotinic acid isopropyl ester | HCID 67027192 | — |
| Product | HCID 67026905 | HCID 67026905 | — |
Reaction Steps
A solution of 2-(1-ethyl-propyl)-6-methyl-isonicotinic acid isopropyl ester (1.54 g, 6.18 mmol) in 25% aq. HCl (60 mL) is stirred at 65° C. for 16 h. The solvent is removed in vacuo and the residue is dissolved in dioxane and concentrated again to give 2-(1-ethyl-propyl)-6-methyl-isonicotinic acid hydrochloride (1.70 g) as a brownish solid; LC-MS: tR=0.62 min, [M+1]+=208.52.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580824B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-a0949b5dd56b40cabc6f3b740feed326 |
| Source note | uspto-grants-2013_11 |