HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(3-Chlorophenyl)prop-2-ynal oxime → 3-(3-Chlorophenyl)-N-hydroxy-prop-2-ynimidoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(3-Chlorophenyl)prop-2-ynal oxime | HCID 76543056 | — |
| Reactant | N-Hydroxy-3-trimethylsilyl-prop-2-ynimidoyl chloride | HCID 86662874 | — |
| Product | 3-(3-Chlorophenyl)-N-hydroxy-prop-2-ynimidoyl chloride | HCID 86662875 | 96.4% |
Reaction Steps
The title compound was prepared following the method herein described for Compound 3b, using Compound 31e instead of 3-trimethylsilylprop-2-ynal oxime. The pale brown residue was used in the next step without further purification. Yield: 96.4%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580962B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-03511dc42bd04cd281104ee0cfc30fe2 |
| Source note | uspto-grants-2013_11 |