HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Phenylethynyl)-1-oxa-2,8-diazaspiro[4.5]dec-2-ene → HCID 57493844, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Phenylethynyl)-1-oxa-2,8-diazaspiro[4.5]dec-2-ene | HCID 57493808 | — |
| Reactant | HCID 57493843 | HCID 57493843 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 57493844 | HCID 57493844 | 33.4% |
Reaction Steps
The title compound was synthesized following the method reported for Compound 1c, substituting Compound 1b with Compound 40a and running the reaction in chloroform. The crude brownish oily residue was used without further purification in the next reaction step. Yield: 33.4%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580962B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-b3dbb826cef843febde5e66b9d16f62d |
| Source note | uspto-grants-2013_11 |