HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butanaminium, N,N,N-tributyl-, fluoride, hydrate → HCID 57493850, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butanaminium, N,N,N-tributyl-, fluoride, hydrate | HCID 16211673 | — |
| Reactant | HCID 57493823 | HCID 57493823 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 57493850 | HCID 57493850 | — |
Reaction Steps
A solution of Compound 28b (557 mg, 1.81 mmol) and tetrabutylammonium fluoride hydrate (759 mg, 2.72 mmol) in 10 mL of THF was stirred at r.t. for 4 h. After the usual work-up with EtOAc-water the crude residue was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580962B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-b5e16263c1dd4dd2a08d7d9c931ad0c5 |
| Source note | uspto-grants-2013_11 |