反应详情

The title compound was prepared following the method reported here for Compound 31a. As starting material spiro[4.5]decan-8-one replaced 1,4-dioxaspiro[4.5]decan-8-one. After the usual work-up procedure, the residue was purified by means of automated flash chromatography (SP01®M-Biotage; CH2Cl2) to give the title compound as a colorless oil. Yield: 98.5%.

1. customThe title compound was prepared
2. customAfter the usual work-up procedure, the residue was purified by means of automated flash chromatography (SP01®M-Biotage; CH2Cl2)