HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3,3-Diethoxyprop-1-yn-1-yl)-3-methylbenzene → 3-(m-Tolyl)propiolaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3,3-Diethoxyprop-1-yn-1-yl)-3-methylbenzene | HCID 10798873 | — |
| Reactant | 3-(3-Chlorophenyl)-2-propynal | HCID 46872540 | — |
| Product | 3-(m-Tolyl)propiolaldehyde | HCID 10773101 | — |
Reaction Steps
The title compound was synthesized following the procedure reported for Compound 31d, but starting from Compound 91a instead of Compound 31c. The crude title compound was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580962B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-0ac243aaa1b841659bffd022b0fab313 |
| Source note | uspto-grants-2013_11 |