HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Hydroxy-3-trimethylsilyl-prop-2-ynimidoyl chloride → N-hydroxy-3-(m-tolyl)prop-2-ynimidoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Hydroxy-3-trimethylsilyl-prop-2-ynimidoyl chloride | HCID 86662874 | — |
| Reactant | N-hydroxy-3-(3-methylphenyl)prop-2-yn-1-imine | HCID 86662876 | — |
| Product | N-hydroxy-3-(m-tolyl)prop-2-ynimidoyl chloride | HCID 86662877 | 96.4% |
Reaction Steps
The title compound was prepared following the method herein described for Compound 3b, using Compound 91c instead of 3-trimethylsilylprop-2-ynal oxime. The residue was used in the next step without further purification. Yield: 96.4%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580962B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-9aba6ff3f2f147f7b09a5ba1475bd47a |
| Source note | uspto-grants-2013_11 |