HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57493780, compound → HCID 76384278, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57493780 | HCID 57493780 | — |
| Reactant | HCID 76384212 | HCID 76384212 | — |
| Product | HCID 76384278 | HCID 76384278 | 82% |
Reaction Steps
The title product was obtained the method described for the compound of Example 84 starting from the Compound of example 93 instead of the compound of Example 83. After the usual work-up procedure, the residue was purified by means of automated flash chromatography (SP01®TM-Biotage; gradient Petroleum Ether-EtOAc from 95:5 to 1:1) to give the title compound as a yellowish oil. Yield: 82%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580962B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-c03cffa9628c49ae85d5bc3e6c5811b7 |
| Source note | uspto-grants-2013_11 |