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HRID2040893

反应详情

EQUATION

反应方程式

HRID 2040893 的结构方程式

REACTANTS

反应物

2
结构：C=C1CC2(CCC2)C1
HCID57493859

未命名化合物

结构：ON=CC#Cc1cccc(Cl)c1
HCID76543056

未命名化合物

PRODUCTS

生成物

1
结构：Clc1cccc(C#CC2=NOC3(C2)CC2(CCC2)C3)c1
HCID56644647

未命名化合物

PROCEDURE

实验过程

The title compound was prepared following the procedure described for Compound 3c, using Compound 31e instead of Compound 3b and Compound 97a instead of Compound 3a. After the usual work-up procedure, the residue was purified by means of automated flash chromatography (SP01®TM-Biotage; Petroleum Ether-EtOAc 97:3; then DCM 100%) to give the title compound as a white-yellowish solid. Yield: 20.7%.

WORKUP

后处理

  1. customThe title compound was prepared
  2. customAfter the usual work-up procedure, the residue was purified by means of automated flash chromatography (SP01®TM-Biotage