HRID2040908

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CON(C)C(=O)N1CCC2(CC(C#Cc3cccc(Cl)c3)=NO2)C1

HCID57493799

未命名化合物

HCID57493822

未命名化合物

PRODUCTS

生成物

结构：CON(C)C(=O)N1CCC2(CC1)CC(C#Cc1cccc(Cl)c1)=NO2

HCID57493794

未命名化合物

收率 74%

PROCEDURE

实验过程

The title compound was synthesized using the method described for the compound of Example 110, replacing Compound 22c for Compound 27d. After evaporation, the crude was purified by means of automated flash chromatography (Isolera®TM-Biotage; gradient petroleum ether-EtOAc 8:2 to 6:4) to afford a pale yellow oil. Yield: 74%.

WORKUP

后处理

customAfter evaporation
customthe crude was purified by means of automated flash chromatography (Isolera®TM-Biotage; gradient petroleum ether-EtOAc 8:2 to 6:4)
customto afford a pale yellow oil