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HRID2041377

反应详情

EQUATION

反应方程式

HRID 2041377 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)N
HCID6385

tert-Butylamine

C4H11N

结构：CC(C)(C)OC(=O)N1CCc2ccc(Cl)c(SCc3ccc(C(=O)O)cn3)c2CC1
HCID57656258

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)NC(=O)c1ccc(CSc2c(Cl)ccc3c2CCNCC3)nc1.Cl
HCID66706857

未命名化合物

PROCEDURE

实验过程

Use a method similar to the Example 375, using 3-tert-butoxycarbonyl-6-(5-carboxy-pyridin-2-ylmethylthio)-7-chloro-2,3,4,5-tetrahydro-1H-benzo[d]azepine and tert-butylamine to give, after deprotection by the General Procedure 1-4, the title compound as an off-white solid. MS (APCI+) m/z: 404 (M+H)+.

WORKUP

后处理

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