Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Boron Trichloride | HCID 25135 | — |
| Reactant | 2-vinylaniline | HCID 10351689 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 59583108 | HCID 59583108 | — |
Reaction Steps
BCl3 (67.8 mL, 1.0 M in hexanes) was added to a solution if 2-vinylaniline (5.3 g, 44.3 mmol) in 40 mL of anhydrous toluene at 0° C. The mixture was stirred at 0° C. for 1 h and then refluxed for 2 h. The mixture was then evaporated to dryness and used immediately for next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08586203B2 |
|---|
| Source dataset | uspto-grants-2013_11 |
|---|
| ORD ID | ord-761626004add4bf7b6f504c4a94321e8 |
|---|
| Source note | uspto-grants-2013_11 |
|---|
