HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 68432550, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 5-fluoro-1-(3-fluorobenzyl)-1H-indole-2-carboxylic acid | HCID 57431513 | — |
| Reactant | HCID 57431528 | HCID 57431528 | — |
| Product | HCID 68432550 | HCID 68432550 | — |
Reaction Steps
The process is carried out according to the method described in step 5.3, using 0.3 g (1.04 mmol) of 5-fluoro-1-(3-fluorobenzyl)-1H-indole-2-carboxylic acid (example 1.1), and of 0.363 g (1.36 mmol) of 6-(pyrrolidin-1-yl)-4-trifluoromethyl-3-aminopyridine hydrochloride, prepared in step 11.4, in the presence of 0.22 ml (1.57 mmol) of triethylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08586573B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-a4e850abe702474399aaa023809716f7 |
| Source note | uspto-grants-2013_11 |