4-Chlorobenzoic Acid → HCID 178523699, compound

Participants

Reaction Steps

The title compound, off-white solid (103 mg, 88%), MS (ISP) m/z=469.3 [(M+H)+], mp 226.5° C., was prepared in accordance with the general method of example 32 from trans-4-{2-[4-(2,3-dihydrofuro[3,2-c]pyridin-4-yl)-piperazin-1-yl]-ethyl}-cyclohexanamine trihydrochloride (intermediate C) (110 mg, 0.25 mmol) and 4-chlorobenzoic acid.

Provenance & Evidence