HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 178474982, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | HCID 178447389 | HCID 178447389 | — |
| Product | HCID 178474982 | HCID 178474982 | — |
Reaction Steps
The title compound, white solid (96 mg, 83%), MS (ISP) m/z=387.4 [(M+H)+], mp 217.5° C., was prepared in accordance with the general method of example 32 from trans-4-{2-[4-(6-methyl-2,3-dihydro-furo[3,2-c]pyridin-4-yl)-piperazin-1-yl]-ethyl}-cyclohexylamine trihydrochloride (intermediate E) (136 mg, 0.3 mmol) and acetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08586579B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-d6db5e0b51a340f5826efb72b252326e |
| Source note | uspto-grants-2013_11 |