HuagongsheHuagongshe Chemistry Print Report · For research reference only
1H-Azepine → 5-[4-(3-Azepan-1-yl-propoxy)-phenyl]-2-methyl-2H-pyridazin-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1H-Azepine | HCID 6451476 | — |
| Reactant | 5-[4-(3-chloropropoxy)-phenyl]-2-methyl-2H-pyridazin-3-one | HCID 56946303 | — |
| Product | 5-[4-(3-Azepan-1-yl-propoxy)-phenyl]-2-methyl-2H-pyridazin-3-one | HCID 24995996 | — |
Reaction Steps
This compound was prepared as the hydrochloride salt using 5-[4-(3-chloropropoxy)-phenyl]-2-methyl-2H-pyridazin-3-one and azepine using the procedure described in Example 91 Step 5; Mp 247-8° C.; MS m/z 342 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08586588B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-428058c0a6a9450984ebff7a82f97faa |
| Source note | uspto-grants-2013_11 |