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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2042597Generated: November 1, 2026

HCID 59652062, compound → HCID 59651940, compound

https://huagongshe.com/reaction/2042597

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 59652062HCID 59652062—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 59651940HCID 59651940—

Reaction Steps

The product from step 1 (1.25 g, 3.83 mmol) and 10% Pd/C (0.3 g) in MeOH (50 mL) was hydrogenated on a Parr apparatus until TLC indicated completion of the reaction. The mixture was filtered, concentrated to an oil and used directly in the next step; MS m/z 204 (M-OMe).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08586588B2
Source datasetuspto-grants-2013_11
ORD IDord-545c26808be14429afabb4d728dbb7e6
Source noteuspto-grants-2013_11