HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59652050, compound → HCID 59652065, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59652050 | HCID 59652050 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 59652065 | HCID 59652065 | 144.2% |
Reaction Steps
In a 10 mL round bottom flask, 4-[3-fluoro-4-(6-oxo-1,4,5,6-tetrahydro-pyridazin-3-yl)-phenoxy]-piperidine-1-carboxylic acid tert-butyl ester (410 mg, 1.0 mmol) in trifluoroacetic acid (3 mL) was stirred 2 h. The solvent concentrated under vacuum to produce 420 mg (100%) of the salt as an oil. MS m/z=292 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08586588B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-163af5966fcd44ffb5fa8bad002c37e9 |
| Source note | uspto-grants-2013_11 |