Ammonium Hydroxide → HCID 178471768, compound

Participants

Reaction Steps

Ammonium hydroxide (large excess) was added to the product from Example 1C (8.43 g. 27.3 mmol) at room temperature. White solids precipitated out and were collected by filtration and washed with water to afford the title compound (7.9 g, 100%) as a white solid which was taken on to the next step-without further purification. MS (DCI) m/z 290.1 [M+H]+.

Provenance & Evidence