HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylethylamine → HCID 53253205, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylethylamine | HCID 11723 | — |
| Reactant | HCID 53252573 | HCID 53252573 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 53253205 | HCID 53253205 | — |
Reaction Steps
Synthesis worked according to the preparation of A7-1 when using 21 mg (0.06 mmol) (R)—N-(8-methoxytetralin-2-yl)-N-propyl-N-[2-(2-thienyl)ethyl]amine ((R)-A5-1: R═OMe, Cy=2-thienyl). Flash chromatography was done using hexane/ethyl acetate 40/10 in the presence of 0.5% (v/v) dimethylethylamine to achieve compound 1a.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08586603B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-573448eb4d2c48b1a0dce64e027d6293 |
| Source note | uspto-grants-2013_11 |