HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 178521146, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 178525710 | HCID 178525710 | — |
| Product | HCID 178521146 | HCID 178521146 | — |
Reaction Steps
trans-4-Trifluoromethyl-cyclohexanecarboxylic acid (2.0 g, 10.2 mmol) is stirred in thionyl chloride (30 mL) for 1 h at reflux. The reaction mixture is concentrated and used directly in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08586604B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-b2d469e03cd04b0c9d6aca5dca3aa72b |
| Source note | uspto-grants-2013_11 |