HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 131731048, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 131731049 | HCID 131731049 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 131731048 | HCID 131731048 | — |
Reaction Steps
To a magnetically stirred solution of MeO-GlyLys [ε-CBz] [α-Lys] [Boc]2 (1.0 g, 1.47 mmol), methanol (32 ml) and water (16 ml) was added 1M aq. NaOH solution (3 ml) at room temperature. The reaction and product isolation were carried out according to the method described in Example 13.vi to afford HO-GlyLys [ε-CBz] [α-Lys] [Boc]2 (942 mg, 96%) as a colourless foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08586705B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-3063750e9db8436cbd8b1f7f2f5dba96 |
| Source note | uspto-grants-2013_11 |