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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2043567Generated: November 2, 2026

Methanol → HCID 131731048, compound

https://huagongshe.com/reaction/2043567

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantSodium HydroxideHCID 14798—
ReactantHCID 131731049HCID 131731049—
SolventWaterHCID 962—
ProductHCID 131731048HCID 131731048—

Reaction Steps

To a magnetically stirred solution of MeO-GlyLys [ε-CBz] [α-Lys] [Boc]2 (1.0 g, 1.47 mmol), methanol (32 ml) and water (16 ml) was added 1M aq. NaOH solution (3 ml) at room temperature. The reaction and product isolation were carried out according to the method described in Example 13.vi to afford HO-GlyLys [ε-CBz] [α-Lys] [Boc]2 (942 mg, 96%) as a colourless foam.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08586705B2
Source datasetuspto-grants-2013_11
ORD IDord-3063750e9db8436cbd8b1f7f2f5dba96
Source noteuspto-grants-2013_11