HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2045017Generated: October 30, 2026
4-Chloro-3-nitrobenzenesulfonamide → HCID 67126605, compound
https://huagongshe.com/reaction/2045017
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Chloro-3-nitrobenzenesulfonamide | HCID 7324 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 67227314 | HCID 67227314 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 67126605 | HCID 67126605 | — |
Reaction Steps
A mixture of 4-chloro-3-nitrobenzenesulfonamide, 4-(aminomethyl)tetrahydro-2H-pyran-4-amine bis-hydrochloric acid salt and triethylamine in dioxane (10 mL) was heated at 110° C. overnight. After cooling, the reaction mixture was diluted with water (10 mL), and the solid was filtered to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08586754B2 |
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| Source dataset | uspto-grants-2013_11 |
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| ORD ID | ord-ff449a6d15fe4c309b809f5b14c0efc3 |
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| Source note | uspto-grants-2013_11 |
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