HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosuccinimide → HCID 67226591, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | HCID 67144445 | HCID 67144445 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 67226591 | HCID 67226591 | — |
Reaction Steps
A mixture of EXAMPLE 400D (0.5 g) and 1-chloropyrrolidine-2,5-dione (0.126 g) in acetonitrile (10 mL) was stirred at room temperature for 4 hours. The solvent was removed, and the residue was purified by flash column chromatography on silica gel to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08586754B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-2b239df6f8d245d58714c36c8fa0867b |
| Source note | uspto-grants-2013_11 |