Sodium Hydroxide → HCID 131731052, compound

HRID 2045681Notes

Reaction equation

HRID 2045681 reaction equation
[Na].[C:2]([OH:21])(=[O:20])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH:17]([CH3:19])[CH3:18].[N+]([O-])([O-])=O.[Ag+:26].[OH-].[Na+].C([O-])(=O)CCCCCCCCCCCCCCC(C)C.[Na+]>O>[C:2]([O-:21])(=[O:20])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH:17]([CH3:18])[CH3:19].[Ag+:26]

Participants

7

Reactant 5

HCID 14798Sodium HydroxideHCID 2185916-Methylheptadecanoic Acid2×HCID 24470Silver Nitrate2×HCID 5360545SodiumHCID 23668820Sodium isooctadecanoate2×

Product 1

HCID 131731052HCID 131731052, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

AgISt was synthesized by the cation exchange reaction of sodium salt of isostearic acid and silver nitrate. 2.85 g of isostearic acid (10 mmol), 0.4 g of sodium hydroxide (10 mmol), and 100 ml triply-distilled water were well mixed at 70° C. for 30 min, then a clear solution containing sodium isostearate was formed. To this sodium isostearate solution, 100 ml of aqueous solution of silver nitrate (1.7 g, 10 mmol) was added dropwise. The yielded AgISt powders were collected, washed, and then dried under reduced pressure at 40° C. for 24 h.

Workup

  1. additionwere well mixed at 70° C. for 30 min
  2. customwas formed
  3. customThe yielded AgISt powders were collected
  4. washwashed
  5. customdried under reduced pressure at 40° C. for 24 h.

Sources & evidence

ORD record
ord-1d54e4f8aadd4a2bad24fee20241172d
Source dataset
uspto-grants-2013_11
Patent number
US08591624B2

Reaction notes

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