HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Acetate → HCID 59606521, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | HCID 86648150 | HCID 86648150 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59606521 | HCID 59606521 | — |
Reaction Steps
9.4 g (6-chloro-4-piperazin-1-yl-pyridazin-3-yl)-dimethylamine hydrochloride and 7.3 g sodium acetate are suspended in 150 ml of methanol and hydrogenated with 1 g Pd/C 10% at ambient temperature. The catalyst is suction filtered, the filtrate is evaporated to dryness and the product is extracted with chloroform and washed with sodium hydroxide solution.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08592400B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-e3aa7f144dfe42b3bd7532b0857bcaaf |
| Source note | uspto-grants-2013_11 |