HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → Di-Tert-Butyl Iodomethyl Phosphate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Di-tert-butyl (chloromethyl) phosphate | HCID 11701630 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | Di-Tert-Butyl Iodomethyl Phosphate | HCID 58196853 | — |
Reaction Steps
The title compound was prepared by halogen exchange reaction of di-tert-butyl chloromethyl phosphate (Intermediate 1) with sodium iodide in suitable solvent such as dry acetone or acetonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08592398B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-5d0d065177be489e8018d0a8042b788f |
| Source note | uspto-grants-2013_11 |